4265-16-1, Benzo[b]furan-2-carboxaldehyde is a benzofuran compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Method B Benzofuran-2-carboxaldehyde (10.0 g, 68 mmol) was dissolved in methanol (70 mL) and cooled to 5 C. Sodium borohydride (2.58 g, 68 mmol) was charged portionwise at 5 C. The batch was aged at 5 C. for 40 minutes and allowed to warm to room temperature (22 C.). The reaction was judged complete by tlc (4:1 hexanes/EtOAc) and the reaction mixture was cooled to 5 C. DI water (20 mL) was charged and the solution was concentrated in vacuo. EtOAc (80 mL) was charged and the solution was washed with DI water (2*20 mL). The EtOAc layer was concentrated in vacuo to provide benzofuran-2-carbinol as an oil.
4265-16-1, The synthetic route of 4265-16-1 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Merck & Co., Inc.; US6071916; (2000); A;,
Benzofuran – Wikipedia
Benzofuran | C8H6O – PubChem