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The present invention provides a novel organophosphoric acid ester represented by the following formula, a process for its production and a pesticidal composition containing this ester as an active ingredient: STR1 where R1 is an alkyl group, R2 is an alkyl group or a thioalkyl group, each of R3, R4 and R5 is a hydrogen atom, a halogen atom, an alkylthio group, a nitro group, a cyano group, an alkyl group, an alkylsulfinyl group, an alkylsulfonyl group or a trifluoromethyl group, and X is an oxygen atom or a sulfur atom.

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Reference:
Benzofuran – Wikipedia,
Benzofuran | C8H2300O – PubChem

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The competitive degradation of six carbamate insecticides by membrane anodic Fenton treatment (AFT), a new Fenton treatment technology, was carried out in this study. The carbamates studied were dioxacarb, carbaryl, fenobucarb, promecarb, bendiocarb, and carbofuran. The results indicate that AFT can effectively degrade these insecticides in both single component and multicomponent systems. The carbamates compete for hydroxyl radicals, and their kinetics obey the previously developed AFT kinetic model quite well. Hydroxyl radical reaction rate constants were obtained, and they decrease in the following order: dioxacarb ? carbaryl > fenobucarb > promecarb > bendiocarb > carbofuran. The AFT is shown to have higher treatment efficiency at higher temperature. Degradation products of the carbamates were determined by gas chromatography/mass spectrometry, and it appears that degradation can be initiated by hydroxyl radical attack at different sites in the molecule, depending on the individual structure of the compound. Substituted phenols are the commonly seen degradation products. The AFT treatment can efficiently remove the chemical oxygen demand of the carbamate mixture, significantly increasing the biodegradability. Earthworm studies show that the AFT is also an effective detoxification process.

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Reference:
Benzofuran – Wikipedia,
Benzofuran | C8H2427O – PubChem

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In view of the wide applicability and versatility of titanium based Lewis acids in selective organic synthesis including asymmetric synthesis, we have synthesized a family of mono and polyatomic titanium derivatives. The polymetallic complexes prepared are bridged by pyridimine, quinone and triazine based ligands. The synthesis of [{Ti(O-i-Pr)3(Oddbf)}2] (1), [Ti(O-i-Pr)2(Oddbf)2] (2), [{Ti(O-i-Pr)2(Oddbf)(OMent)}2] (3) (ddbfO = 2,3-dihydro-2,2-dimethyl-benzofuranoxo; MentO = (1R,2S,5R)-(-)-menthoxo), [{Ti(O-i-Pr)3(OMenpy)}2] (4), [Ti(O-i-Pr)2(OMenpy)2] (5) (MenpyO = (1S,2S,5R)-(-)-menthoxo-pyridine); [{(Ti(OR)3)2L}n] (RO = isopropoxo, (1R,2S,5R)-(-)-menthoxo) (6-11) and [{(Ti(O-i-Pr)3)3L}n] (12) was accomplished from a Lewis acid such as Ti(O-i-Pr)4, [{Ti(O-i-Pr)3(OMent)}2] or [Ti(OMent)4] and chelating ligands (ddbfOH = 2,3-dihydro-2,2-dimethyl-benzofuranol; MenpyOH = (1R,2S,5R)-(-)-5-methyl-2-isopropyl-1-(2?-pyridinyl)cyclohexan-1-o l; LH2 = 4,6-dihydroxy-2,5-diphenyl-pyrimidine, 2,4-dihydroxy-5,6-dimethyl-pyrimidine, 5,8-dihydroxy-1,4-napthoquinone, 2,5-dihydroxy-1,4-benzoquinone and LH3 = cyanuric acid) that provide a rigid framework for the metal centre. The molecular structure of 5 has been determined by single crystal X-ray diffraction studies.

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Reference:
Benzofuran – Wikipedia,
Benzofuran | C8H2397O – PubChem

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The potential of liquid chromatography quadrupole time-of-flight mass spectrometry (LC-QqTOF-MS) to identify and confirm carbosulfan and seven of its main metabolites (carbofuran, 3-hydroxycarbofuran, 3-ketocarbofuran, 3-hydroxy-7-phenol carbofuran, 3-keto-7-phenolcarbofuran, 7-phenolcarbofuran, dibutylamine) at trace levels from food is explored for the first time. The analytical method developed consists of pressurized liquid extraction (PLE) and LC-QqTOF-MS in positive ion mode, which attains unequivocal identification and quantification of the studied compounds in food, at levels well below of those of concern (0.05 mg/kg for the sum of carbosulfan, carbofuran, and 3-hydroxycarbofuran). PLE recoveries ranged from 55 to 94% with limits of quantification from 10 (for carbosulfan, carbofuran, 3-hydroxycarbofuran, and dibutylamine) to 70 mug/kg (3-keto-7-phenolcarbofuran). The method is precise, with relative standard deviations varying between 5 and 11% for the repeatability (within-day) and 8-13% for the reproducibility (interday). This method was used to monitor the presence and fate of the target compounds in orange, potato, and rice crops treated with a commercial product containing carbosulfan. Field degradation studies show that carbofuran, 3-hydroxycarbofuran, and dibutylamine are the main degradation products formed in the environmental disappearance of carbosulfan.

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Reference:
Benzofuran – Wikipedia,
Benzofuran | C8H2416O – PubChem

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BRD4, characterized by two acetyl-lysine binding bromodomains and an extra-terminal (ET) domain, is a key chromatin organizer that directs gene activation in chromatin through transcription factor recruitment, enhancer assembly, and pause release of the RNA polymerase II complex for transcription elongation. BRD4 has been recently validated as a new epigenetic drug target for cancer and inflammation. Our current knowledge of the functional differences of the two bromodomains of BRD4, however, is limited and is hindered by the lack of selective inhibitors. Here, we report our structure-guided development of diazobenzene-based small-molecule inhibitors for the BRD4 bromodomains that have over 90% sequence identity at the acetyl-lysine binding site. Our lead compound, MS436, through a set of water-mediated interactions, exhibits low nanomolar affinity (estimated Ki of 30-50 nM), with preference for the first bromodomain over the second. We demonstrated that MS436 effectively inhibits BRD4 activity in NF-kappaB-directed production of nitric oxide and proinflammatory cytokine interleukin-6 in murine macrophages. MS436 represents a new class of bromodomain inhibitors and will facilitate further investigation of the biological functions of the two bromodomains of BRD4 in gene expression.

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Reference:
Benzofuran – Wikipedia,
Benzofuran | C8H2435O – PubChem

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Abstract: Carbofuran residue in vegetables is a concern to human health. Direct competitive enzyme-linked immunosorbent assay (dcELISA) and dipstick immunoassay were developed in the present study. The dcELISA showed a 50% inhibition concentration (IC50) and working range of 1.3 and 0.2 to 7.5 ng/mL, respectively, while the cutoff value of dipstick immunoassay was 20 ng/mL. Applying the two immunoassays, we achieved the goal of rapid screening of carbofuran residue in commercial vegetables with a simple sample processing method. Among 46 leek, 39 potato, and 39 sweet potato samples, carbofuran residue was detected in 22% of the leek samples, and two samples exceeded the maximum residue limit of China (0.02 mg/kg). In addition, carbofuran residue was found at less than 2.5 ng/g in one potato and one sweet potato samples. The residual level of carbofuran measured by immunoassays agreed well with those determined by ultra-performance liquid chromatography tandem mass spectrometry. To ensure food safety and human health, it is greatly necessary and meaningful to monitor carbofuran residue in commercial vegetables. Practical Application: Rapid monitoring of carbofuran residue in vegetables is very necessary and important for consumers, regulatory agencies, and food industry.

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Reference:
Benzofuran – Wikipedia,
Benzofuran | C8H2437O – PubChem

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Cellular immobilisation (CI) is a method characterised by restricting the cells to a delimited area while preserving their metabolic, catabolic, and catalytic activities Biodegradation of contaminants is one of the potential applications of CI. Immobilised cells can achieve to degrade the degradation of toxic substances with higher efficiency than cells in a free state. free cells. The aim of this work was to compile the most important aspects of CI as a strategy for the degradation of pesticides. We discuss the main targeted chemical substances, the used microorganisms, materials, and techniques, as well as their advantages, and limitations We highlight increases in the percentage of degradation, greater stability, protection, and tolerance to pesticides when a CI strategy is implemented. Finally, the requirements for deepening our understanding of the involved kinetic, molecular, and transfer processes are discussed, particularly for their application in situ.

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Reference:
Benzofuran – Wikipedia,
Benzofuran | C8H2350O – PubChem

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This study examined the photodecomposition of carbofuran, a carbamate pesticide with high oral toxicity. Rate constants are measured for the pesticide in aqueous solution and in the presence of various samples of dissolved organic matter (DOM). Kinetic experiments are monitored with HPLC, while reaction products are determined using HPLC, GC-MS, and 1H NMR: mechanisms are proposed for the first three steps of the reaction. It was found that the photodecomposition proceeds via first-order reaction kinetics and that the presence of various DOM samples inhibits the photolysis reaction of carbofuran. This phenomenon can be correlated to the magnitude of the binding interaction between carbofuran and DOM. Finally, techniques such as GC-MS and 1H NMR are used to identify the photodecomposition products. The first three steps of the reaction are defined. In the first step of the reaction, the carbamate group is cleaved from the molecule. The furan moiety is opened in the second step producing a substituted catechol with a tert-butyl alcohol group as the substituent at the number three carbon. This molecule then undergoes a dehydration reaction to form an alkene side group from the tert-butyl alcohol side group.

Sometimes chemists are able to propose two or more mechanisms that are consistent with the available data. Quality Control of 2,2-Dimethyl-2,3-dihydrobenzofuran-7-ol, If a proposed mechanism predicts the wrong experimental rate law, however, the mechanism must be incorrect.Welcome to check out more blogs about 1563-38-8, in my other articles.

Reference:
Benzofuran – Wikipedia,
Benzofuran | C8H2340O – PubChem

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In homogeneous catalysis, the catalyst is in the same phase as the reactant. The number of collisions between reactants and catalyst is at a maximum.In a patent, 1563-38-8, name is 2,2-Dimethyl-2,3-dihydrobenzofuran-7-ol, introducing its new discovery. Recommanded Product: 1563-38-8

After years of influence of titanium-based Ziegler-Natta catalysts on “petropolymers” synthesis, titanium complexes are experiencing a resurgence in research efforts as sustainable catalysts for biopolymer synthesis. This review article summarizes the different classes of well-defined homogeneous and heterogeneous titanium catalysts supported by various multidentate ancillary ligands for the synthesis of polyesters, polycarbonates and poly(methyl metacrylate) derivatives which are biodegradable and/or synthesized from renewable monomers. Special attention is given to the relationships between the electronic and steric effects of catalysts governing the activity, control and stereoselectivity whenever applicable.

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Reference:
Benzofuran – Wikipedia,
Benzofuran | C8H2380O – PubChem

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A process is disclosed for preparing a carbamic acid phenyl ester of the formula (I) STR1 wherein R is alkyl having 1 to 8 carbon atoms, aryl, cycloalkyl having 5 or 6 carbon atoms, or aralkyl having 7 to 16 carbon atoms, wherein the aryl, cycloalkyl or aralkyl is unsubstituted or substituted by at least one alkyl group having 1 to 8 carbon atoms; R1 is hydrogen, alkyl having 1 to 4 carbon atoms, alkoxy having 1 to 4 carbon atoms, cyanomethyl, 1,3-dioxolan-2-yl, or carboalkoxyamino wherein the alkoxy group contains 1 to 4 carbon atoms; R2 is hydrogen, halogen, alkyl having 1 to 4 carbon atoms or alkoxy having 1 to 4 carbon atoms; or R1 and R2 form together a carbocyclic ring or a heterocyclic ring fused to the phenyl ring wherein the carbocyclic ring of the heterocyclic ring is unsubstituted or substituted by at least one alkyl having 1 to 8 carbon atoms, which comprises acylating a phenol of the formula (II) STR2 with a compound of the formula (IV) STR3 in the presence of a base. The compounds obtained are valuable intermediates.

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Reference:
Benzofuran – Wikipedia,
Benzofuran | C8H2317O – PubChem