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Fast pyrolysis of pine sawdust (PS) was investigated in a drop tube quartz reactor to understand the effects of temperature and atmosphere (Ar and H2) on the product yields, gas composition, bio-oil characteristics (organic composition and molecular mass distributions (MMDs)), and the carbon and oxygen conversion. The pyrolysis behavior and typical products from PS pyrolysis were also conducted using a thermogravimetry-mass spectroscopy (TG-MS) and pyrolysis-gas-chromatography/mass spectrometry (Py-GC/MS). The results show that the highest oil yields can be obtained at 500 C of 55.09 and 54.41 wt.% under Ar and H2 atmosphere, respectively. In comparison to an inert atmosphere, H2 created lower oil yields but higher gas yields, especially for CO and CH4 yields, and narrower MMDs, smaller Mn and Mw, and fewer char especially at high temperatures. The high temperatures and H2 atmosphere contribute to the oxygen and carbon transferring from material to volatile, especially to the gaseous products. H2 can promote the secondary cracking of macromolecules and weaken the re-polymerization of anhydrosugar and lignin oligomers.

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Reference：
Benzofuran – Wikipedia,
Benzofuran | C8H2125O – PubChem

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The chemical structure of soil organic matter fractions and its relationship to biological processes remains uncertain. We used pyrolysis-gas chromatography/mass spectrometry to analyze the molecular structure of light and heavy fraction C from soils in the San Juan Mountains, Colorado. The soil samples, each replicated three times, were from two elevations (alpine and low forest) within two geochemically distinct basins (igneous and sedimentary). We also analyzed whether variation in the activity of nine enzymes that mediate soil organic matter turnover and nutrient cycling could explain differences in C structure. We found that, across basins and elevation, light fraction and heavy fraction C had distinct chemistries. The light fraction was characterized by an abundance of plant lignin biomarkers, including phenol, 2-methoxy-4-vinyl-(vinylguaiacol) and phenol, 2-methoxy-(guaiacol); in contrast heavy fraction had very little unaltered lignin but an abundance of polysaccharides, such as furfural, and proteins such as pyrrole. In alpine sites, light fraction was less abundant (4.27 versus 31.79 g kg-1) and had a lower C/N ratio (17.25 versus 32.01) than in forests. The alpine sites also had higher activities of phosphatase, beta-d-1,4-cellobiosidase, beta-1,4-glucosidase, l-leucine aminopeptidase, and beta-1,4-xylosidase. Protein abundance in the heavy fraction was correlated with peptidase, beta-1,4-glucosidase, and phosphatase activities; in the light fraction, protein abundance was correlated with peptidase, xylosidase, and beta-d-1,4-cellobiosidase activities. beta-1,4-N-acetyl-glucosaminidase was negatively correlated with polysaccharides in the light and heavy fractions and positively correlated with lignin in the light fraction. However, there were not always significant correlations between enzymes and substrates. We suggest that this is likely because soil organic matter chemistry reflects long-term decomposition processes while enzyme dynamics fluctuate with current conditions or due to the presence of a pool of sorbed enzymes in the heavy fraction. While alpine and forest ecosystem C distribution and enzyme activities varied, substantial depletion of lignin derivatives in the heavy fraction across sites suggest that these compounds do not persist in stable soil C pools.

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Reference：
Benzofuran – Wikipedia,
Benzofuran | C8H2110O – PubChem

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Pterocarpus is one of the most widely used timber resources on the market. But the utilization rate has been low. In order to improve the utilization of Pterocarpus processing residue, as well as explore the reason of its good decay-resistance. In this study, the antifungal mechanism of Peterocarpes spp., aqueous extracts and ethanol extracts of three Pterocarpus species were studied. The antimicrobial active factors were analyzed by gas chromatography-mass spectrometry. Italian poplar (Populus euramevicana cv. ?I-214?) wood was immersed in the extracts and then inoculated with both Coriolus versicolor and Gloeophyllum trabeum. The antimicrobial properties of the extracts were studied, and the mechanism underlying these properties were analyzed using gas chromatography-mass spectrometry. The results showed that the yield of ethanol extracts from the three Pterocarpus species was significantly higher than that of aqueous extracts. Pterocarpus soyauxii and Pterocarpus macarocarpus produced the highest yield of ethanol extracts (28.59%) and aqueous extracts (14.31%), respectively. With increasing concentrations, the antimicrobial activities of aqueous extracts of Pterocarpus angolensis and Pterocarpus macarocarpus gradually increased, while the antimicrobial activity of other extracts remained constant. Gas chromatography-mass spectrometry analysis identified a considerable number of phenols, ketones, amines, and aromatic compounds in all extracts, which is consistent with their antimicrobial activity and suggests synergism among the chemicals.

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Reference：
Benzofuran – Wikipedia,
Benzofuran | C8H2101O – PubChem

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Despite studies on umbelliferous fruits flavor makeup, nothing is known regarding roasting impact on their fruit aroma. Five major umbelliferous crops viz., anise, caraway, coriander, cumin and fennel were analyzed via headspace solid-phase microextraction to reveal for 117 volatile constituents. Oxygenated monoterpenes amounted for the major volatile class in raw fruits at 75% with (E)-anethole, carvone, beta-linalool, cuminaldehyde and estragole as major components in anise, caraway, coriander, cumin, and fennel, respectively. Difference was observed in fennel fruit ?estragole? levels derived from different origins. Upon roasting, several novel volatiles were detected viz. pyrazines and flavored Milliard type volatiles. Major flavor intensified response was detected in cumin with an increase in its ?cuminaldehyde? levels versus a decrease of estragole levels in fennel. Roasted cumin exhibited highest peroxide value 14.2 mEq O2/Kg, whereas the least was detected in fennel at 6.1 mEq O2/Kg, though with both values not representing a health hazard.

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Reference：
Benzofuran – Wikipedia,
Benzofuran | C8H2107O – PubChem

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Amarone is a wine produced from withered grapes of Corvina, Corvinone, and Rondinella varieties. The berries? water loss in the withering process, combined with berry senescence, results in significant metabolic changes. Here, we report on changes in malic acid, total polyphenols, and aroma compounds of three single Amarone varieties during withering. Grape bunches of the three varieties were withered in a commercial facility, and weight loss (WL) was measured to determine the time of sampling of grapes for analyses (10, 20, 30, and 50% WL). Rondinella grapes lost weight faster than did Corvina and Corvinone grapes. Malic acid decreased rapidly in all varieties, but in Rondinella grapes with 20% WL, malic acid subsequently increased. Total polyphenols rose slightly in grapes with 20% WL, and their content then increased more than could be attributed to concentration effects. At harvest, the aroma compounds that were initially present at high concentrations and decreased during withering were 6-methoxy-3-methylbenzofuran; 4-vinylguaiacol; 3,4,5-trimethoxybenzyl alcohol; vomifoliol; and coumaran, which were detected in all varieties, reaching the highest concentrations in Corvinone. During withering, most of these markers showed a peak at 10% or 20% WL in Rondinella grapes, whereas in Corvinone, they peaked at 20% WL as in Corvina grapes, which also exhibited a concentration peak of some compounds at 30% WL. We conclude that not all grape varieties behave in the same way in withering; therefore, it is necessary that winemakers know the weight loss (and the time) at which the best aromatic expression is reached to determine the optimal processing stage of a variety. By matching malic acid trends with those of aroma compounds, we propose that malic acid could be a useful tool for monitoring the changes in aroma compounds during grape withering.

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Reference：
Benzofuran – Wikipedia,
Benzofuran | C8H2104O – PubChem

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The Reaction of 2,3-Dichloro-5,6-dicyano-p-benzoquinone with Benzofurans and Indoles

The reaction of 2,3-dichloro-5,6-dicyano-p-benzoquinone (DDQ) with 6-methoxy-3-methylbenzofuran gave carbon-oxygen adduct.The reaction in less polar solvents such as benzene and CH2Cl2 proceeds faster than that in more polar solvents such as THF and dioxane.In contrast, the reaction of DDQ with indoles gave carbon-carbon adducts.This reaction proceeds rapidly with increasing solvent polarity.

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Benzofuran – Wikipedia,
Benzofuran | C8H2123O – PubChem

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Electric Literature of 29040-52-6, Catalysts function by providing an alternate reaction mechanism that has a lower activation energy than would be found in the absence of the catalyst. In some cases, the catalyzed mechanism may include additional steps.In a article, 29040-52-6, molcular formula is C10H10O2, introducing its new discovery.

Performance of a conical spouted bed pilot plant for bio-oil production by poplar flash pyrolysis

Poplar (Populus nigra) flash pyrolysis has been performed at the IK4-Ikerlan 25 kg h-1 pilot plant equipped with a conical spouted bed reactor. Gas, bio-oil and char yields and properties have been studied in the 425-525 C range. This reactor has been proven to be especially suitable for this process as high bio-oil yields have been obtained, with the maximum being 69 wt.% at 455 C. The bio-oil has been collected in two fractions: the lighter one, which accounts for 85 wt.% of the bio-oil, has a high water content and is composed mainly of acids and ketones, whereas the heavier fraction has a lower water content and is rich in phenols. These fractions are miscible, obtaining a bio-oil with a water content lower than 25 wt.% and a higher heating value in the 16-18 MJ kg-1 range.

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Benzofuran – Wikipedia,
Benzofuran | C8H2117O – PubChem

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The effect of biomass pretreatment on catalytic pyrolysis products of pine wood by Py-GC/MS and principal component analysis

Non-catalytic and catalytic pyrolysis of pretreated pine wood was conducted using pyrolysis-gas chromatography/mass spectrometry (Py-GC/MS). Biomass pretreatment included acid-leaching, torrefaction, and acid-leaching followed by torrefaction. Forty-five pyrolysis products were identified in the Py-GC/MS chromatograms and their peak area data evaluated by principal component analysis. In non-catalytic pyrolysis, acid-leaching pretreatment enhanced the levels of levoglucosan, while torrefaction pretreatment enhanced the proportion of catechols in the volatile products. Increasing both the temperature and catalyst loading in catalytic pyrolysis promoted the formation of aromatic hydrocarbons. At lower pyrolysis temperatures (450?500 C), acid-leaching pretreatment resulted in slightly lower proportions of aromatics, while torrefaction pretreatment had the opposite effect. Overall, temperature and catalyst loading were considerably more important factors in catalytic fast pyrolysis of pine wood than biomass pretreatment as studied by Py-GC/MS.

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Reference£º
Benzofuran – Wikipedia,
Benzofuran | C8H2127O – PubChem

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BCl3-promoted synthesis of benzofurans

Lewis acidic nature of boron trichloride (BCl3) to coordinate to the carbonyl functionality was exploited for the synthesis of benzofurans via dehydrative cyclization. This mild and efficient procedure allowed for facile access to a number of highly substituted benzofurans in a regioselective manner. The structural requirement for the successful cyclodehydration was examined in the cases, where competitive demethylation could occur.

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Benzofuran – Wikipedia,
Benzofuran | C8H2113O – PubChem

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Discovery of 4,6-bis(benzyloxy)-3-phenylbenzofuran as a novel Pin1 inhibitor to suppress hepatocellular carcinoma via upregulating microRNA biogenesis

Peptidyl-prolyl cis-trans isomerase NIMA-interacting 1 (Pin1)participates in diverse cancer-associated signaling pathways, playing an oncogenic role in multiple human cancers, including hepatocellular carcinoma (HCC). Our recent works clarify that Pin1 modulates miRNAs biogenesis by interacting with ERK-phosphorylated exportin-5 (XPO5)and changing XPO5 conformation, giving a potential target for HCC treatment. Herein, we discover 4,6-bis(benzyloxy)-3-phenylbenzofuran (TAB29)as a novel Pin1 inhibitor that targets Pin1 PPIase domain. TAB29 potently inhibits Pin1 activity with the IC50 value of 874 nM and displays an excellent selectivity toward Pin1 in vitro. Cell-based biological evaluation reveals that TAB29 significantly suppresses cell proliferation of HCC cells through restoring the nucleus-to-cytoplasm export of XPO5 and upregulating mature miRNAs expression. Collectively, this work provides a promising small molecule lead compound for Pin1 inhibition, highlighting the therapeutic potential of miRNA-based treatment for human cancers.

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Benzofuran – Wikipedia,
Benzofuran | C8H2108O – PubChem