13391-28-1, 5-Methoxybenzofuran is a benzofuran compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated,13391-28-1
General procedure: To a solution of 14a (or 14b) (2 mmol) in anhydrous chlorobenzene (20 mL) a solution of BBr3SMe2 1M in CH2Cl2 (4 mL, 4 mmol) was added dropwise at 0C and under Ar atmosphere. The reaction was kept stirring at reflux for 10h. After cooling down, the reaction was quenched with water and extracted with CH2Cl2 (three times). The organic layers were collected, dried with anhydrous Na2SO4, filtered and concentrated in vacuo. The crude was purified on silica gel to afford compounds 9a (or 9b) with 80% (or 81%) yield. 1H and 13C spectra of compounds 9a-b were in agreement with literature data.[1]
13391-28-1 5-Methoxybenzofuran 25943, abenzofuran compound, is more and more widely used in various fields.
Reference£º
Article; Tramutola, Francesco; Armentano, Maria Francesca; Berti, Federico; Chiummiento, Lucia; Lupattelli, Paolo; D’Orsi, Rosarita; Miglionico, Rocchina; Milella, Luigi; Bisaccia, Faustino; Funicello, Maria; Bioorganic and Medicinal Chemistry; vol. 27; 9; (2019); p. 1863 – 1870;,
Benzofuran – Wikipedia
Benzofuran | C8H6O – PubChem